C₁₈H₂₄O₅

Base Information

Chemical Name:C₁₈H₂₄O₅
CAS No.:1423021-41-3
Molecular Formula:C₁₈H₂₄O₅
Molecular Weight:320.386
Hs Code.:

C<sub>18</sub>H<sub>24</sub>O<sub>5</sub>

Synonyms:

Suppliers and Price of C₁₈H₂₄O₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₈H₂₄O₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₈H₂₄O₅

There total 16 articles about C₁₈H₂₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1423021-39-9
methyl 2-((1S,4S,5R)-5-((4-methoxybenzyloxy)methyl)-4-methylcyclopent-2-enyl)acetate

: 1423021-41-3
C₁₈H₂₄O₅

: 1423021-43-5
C₁₈H₂₄O₅

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 5h; Overall yield = 84 %; Overall yield = 351 mg; Inert atmosphere;
DOI:10.1002/cjoc.201201039

Reference yield:

(2R,3S,5S)-2-Chloro-3-hydroxy-5-isopropenyl-2-methyl-cyclohexanone: 156714-47-5
(2R,3S,5S)-2-Chloro-3-hydroxy-5-isopropenyl-2-methyl-cyclohexanone

: 1423021-41-3
C₁₈H₂₄O₅

: 1423021-43-5
C₁₈H₂₄O₅

Guidance literature:: Multi-step reaction with 15 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 20 °C / Inert atmosphere

2.1: methanol; diethyl ether / 0 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

4.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / Inert atmosphere

5.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / Inert atmosphere

6.1: sodium periodate / water; acetone / 20 °C / Inert atmosphere

7.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: palladium diacetate; triphenylphosphine; tri-n-butyl-tin hydride / tetrahydrofuran / 20 °C / Inert atmosphere

9.1: dimethylsulfide borane complex / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere

9.2: 3 h / Inert atmosphere

10.1: dipyridinium dichromate / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere

11.1: hydrogen fluoride / water; acetonitrile / 10 h / 20 °C / Inert atmosphere

12.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

12.2: 2 h / Inert atmosphere

13.1: tetrahydrofuran; mineral oil / 10 h / Inert atmosphere

14.1: o-xylene / Inert atmosphere; Reflux

15.1: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane / 5 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; lithium aluminium tetrahydride; dipyridinium dichromate; dimethylsulfide borane complex; hydrogen fluoride; tri-n-butyl-tin hydride; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; o-xylene; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil; 12.1: |Chugaev Elimination Reaction;
DOI:10.1002/cjoc.201201039

Reference yield:

: 1423021-18-4
C₁₆H₂₉ClO₂Si

: 1423021-41-3
C₁₈H₂₄O₅

: 1423021-43-5
C₁₈H₂₄O₅

Guidance literature:: Multi-step reaction with 14 steps

1.1: methanol; diethyl ether / 0 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

3.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / Inert atmosphere

4.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / Inert atmosphere

5.1: sodium periodate / water; acetone / 20 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

6.2: Inert atmosphere

7.1: palladium diacetate; triphenylphosphine; tri-n-butyl-tin hydride / tetrahydrofuran / 20 °C / Inert atmosphere

8.1: dimethylsulfide borane complex / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere

8.2: 3 h / Inert atmosphere

9.1: dipyridinium dichromate / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere

10.1: hydrogen fluoride / water; acetonitrile / 10 h / 20 °C / Inert atmosphere

11.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

11.2: 2 h / Inert atmosphere

12.1: tetrahydrofuran; mineral oil / 10 h / Inert atmosphere

13.1: o-xylene / Inert atmosphere; Reflux

14.1: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane / 5 h / 20 °C / Inert atmosphere

With potassium osmate(VI) dihydrate; sodium periodate; lithium aluminium tetrahydride; dipyridinium dichromate; dimethylsulfide borane complex; hydrogen fluoride; tri-n-butyl-tin hydride; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; o-xylene; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil; 11.1: |Chugaev Elimination Reaction;
DOI:10.1002/cjoc.201201039