3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi

Base Information

Chemical Name:3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi
CAS No.:109057-05-8
Molecular Formula:C₂₇H₂₉Cl₄N₃O₃
Molecular Weight:585.358
Hs Code.:

3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi<isoxazole>

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Chemical Property of 3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi

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Technology Process of 3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi

There total 9 articles about 3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109056-91-9
3-(3,5-Dichloro-2,4,6-trimethylphenyl)-4-methylene-5-morpholino-4,5-dihydroisoxazole

: 13456-86-5
3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide

: 109057-05-8
3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi

Guidance literature:: In chloroform; Ambient temperature;

Reference yield: 84.0%

: 129410-51-1
N-morpholinoallene

: 13456-86-5
3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide

: 109057-05-8
3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi

Guidance literature:: In tetrachloromethane; for 18h; Heating;

Reference yield:

: 5799-76-8
N-propargylmorpholine

: 109057-05-8
3,3'-Di(3,5-dichloro-2,4,6-trimethylphenyl)-5-morpholino-4,5,4',5'-tetrahydro-4,5'-spirobi

Guidance literature:: Multi-step reaction with 5 steps

1: 39 percent / KOtBu / tetrahydrofuran / 0.05 h / 55 °C

2: 1.2 g / 2 h / Heating

3: 57 percent / 2 h / Heating

4: 53 percent / NaOEt / ethanol / 2 h / Heating

5: CCl₄ / Heating

With potassium tert-butylate; sodium ethanolate; In tetrahydrofuran; tetrachloromethane; ethanol;