C₂₂H₂₂O₆

Base Information

Chemical Name:C₂₂H₂₂O₆
CAS No.:1572455-19-6
Molecular Formula:C₂₂H₂₂O₆
Molecular Weight:382.413
Hs Code.:

C<sub>22</sub>H<sub>22</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₂O₆

Chemical Property:

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Technology Process of C₂₂H₂₂O₆

There total 11 articles about C₂₂H₂₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1572455-18-5
C₂₂H₂₄O₆

: 1572455-19-6
C₂₂H₂₂O₆

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃; for 0.99h;
DOI:10.1021/jo500210k

Reference yield:

: 1572455-04-9
C₁₁H₁₇BrO₄

: 1572455-19-6
C₂₂H₂₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid / water / 14 h / 70 °C

2: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 °C

3: diisobutylaluminium hydride / dichloromethane; hexane / 6 h / -78 °C / Inert atmosphere

4: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / water; tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

5: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2.17 h / 18 °C

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 14 h / 0 - 18 °C

7: triethylamine; dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.99 h / -78 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; oxalyl dichloride; diisobutylaluminium hydride; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane; water; 4: |Suzuki-Miyaura Coupling / 5: |Mitsunobu Displacement / 7: |Swern Oxidation;
DOI:10.1021/jo500210k

Reference yield:

: 130669-75-9
(3aS,7aS)-4-bromo-2,2-dimethyl-3a,7a-dihydro-1,3-benzodioxole

: 1572455-19-6
C₂₂H₂₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: osmium(VIII) oxide / water; acetone / 8 h / 18 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

2.2: 1 h / 18 °C

3.1: acetic acid / water / 14 h / 70 °C

4.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 °C

5.1: diisobutylaluminium hydride / dichloromethane; hexane / 6 h / -78 °C / Inert atmosphere

6.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / water; tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

7.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2.17 h / 18 °C

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 14 h / 0 - 18 °C

9.1: triethylamine; dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.99 h / -78 °C

With osmium(VIII) oxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; oxalyl dichloride; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane; water; acetone; mineral oil; 6.1: |Suzuki-Miyaura Coupling / 7.1: |Mitsunobu Displacement / 9.1: |Swern Oxidation;
DOI:10.1021/jo500210k