Technology Process of C21H30O6
There total 7 articles about C21H30O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetyl chloride / 0.08 h / -5 °C / Inert atmosphere
1.2: 100 °C / Inert atmosphere
2.1: AD-mix β; methanesulfonamide; sodium hydrogencarbonate / water; tert-butyl alcohol / 0 °C
3.1: toluene-4-sulfonic acid / 20 °C / Molecular sieve
4.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0 - 30 °C
5.1: manganese(IV) oxide / 1,2-dichloro-ethane / 0.83 h / 62 °C
6.1: lanthanum(lll) triflate / toluene / 2 h / 20 °C
With
manganese(IV) oxide; lithium aluminium tetrahydride; methanesulfonamide; AD-mix β; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetyl chloride; lanthanum(lll) triflate;
In
tetrahydrofuran; diethyl ether; water; 1,2-dichloro-ethane; toluene; tert-butyl alcohol;
2.1: |Sharpless Dihydroxylation / 5.1: |Wittig Olefination;
DOI:10.1002/anie.201402440
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0 - 30 °C
2: manganese(IV) oxide / 1,2-dichloro-ethane / 0.83 h / 62 °C
3: lanthanum(lll) triflate / toluene / 2 h / 20 °C
With
manganese(IV) oxide; lithium aluminium tetrahydride; lanthanum(lll) triflate;
In
tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane; toluene;
2: |Wittig Olefination;
DOI:10.1002/anie.201402440
