Technology Process of C26H30N4O5S
There total 7 articles about C26H30N4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice
1.2: 3 h / 0 - 20 °C / pH 7 - 8
2.1: acetic acid; zinc / 5 h / 20 °C
With
acetic acid; zinc;
In
N,N-dimethyl-formamide;
DOI:10.1021/jm3012917
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydrogensulfate / ethyl acetate
2.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice
2.2: 3 h / 0 - 20 °C / pH 7 - 8
3.1: acetic acid; zinc / 5 h / 20 °C
With
potassium hydrogensulfate; acetic acid; zinc;
In
ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm3012917
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Reflux
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3.58 h / 0 - 20 °C / pH 8 - 9
3.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice
3.2: 3 h / 0 - 20 °C / pH 7 - 8
4.1: acetic acid; zinc / 5 h / 20 °C
With
acetic acid; N-ethyl-N,N-diisopropylamine; zinc;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3012917