3-((2R,3S,12bR)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester

Base Information

• Chemical Name: 3-((2R,3S,12bR)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester
• CAS No.: 88939-25-7
• Molecular Formula: C₂₈H₃₀N₂O₆S
• Molecular Weight: 522.622

Synonyms:

Chemical Property of 3-((2R,3S,12bR)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-((2R,3S,12bR)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester

There total 3 articles about 3-((2R,3S,12bR)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

methyl 2-phenylsulfinylacetate (14090-83-6) + Acetic acid (2S,12bS)-3-methylene-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-ylmethyl ester (78229-29-5) → 3-((2S,12bS)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester (88939-25-7,88980-43-2)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; for 48h; Ambient temperature;

DOI:10.1016/S0040-4020(01)88605-1

Reference yield:

methyl 2-phenylsulfinylacetate (14090-83-6) + Acetic acid (2S,12bS)-3-methylene-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-ylmethyl ester (78229-29-5) → 3-((2R,3R,12bR)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester (88939-25-7,88980-43-2)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; for 48h; Yield given; Ambient temperature;

DOI:10.1016/S0040-4020(01)88605-1

Reference yield:

methyl 2-phenylsulfinylacetate (14090-83-6) + Acetic acid (2S,12bS)-3-methylene-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-ylmethyl ester (78229-29-5) → 3-((2R,3S,12bR)-2-Acetoxymethyl-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-3-yl)-2-benzenesulfinyl-propionic acid methyl ester (88939-25-7,88980-43-2)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; for 48h; Yield given; Ambient temperature;

DOI:10.1016/S0040-4020(01)88605-1

upstream raw materials:

methyl 2-phenylsulfinylacetate

Acetic acid (2S,12bS)-3-methylene-4-oxo-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-ylmethyl ester

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