(+)-MBDB

Base Information

• Chemical Name: (+)-MBDB
• CAS No.: 103882-54-8
• Molecular Formula: C₁₂H₁₇NO₂
• Molecular Weight: 207.272

Synonyms:

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Chemical Property of (+)-MBDB

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+)-MBDB

There total 5 articles about (+)-MBDB which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S,S)-(-)-N-1-phenethyl-1-(1,3-benzodioxol-5-yl)-2-butanamine hydrochloride → (+)-MBDB (103882-54-8,103818-46-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 91.9 percent / H₂ / 10percent Pd/C / methanol; H₂O / 48 h / 2585.7 Torr

2: Heating

3: LAH / diethyl ether / 4 h / Heating

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In methanol; diethyl ether; water;

DOI:10.1021/jm00160a035

Reference yield:

(4S,5R)-5-Benzo[1,3]dioxol-5-yl-4-ethyl-3-methyl-oxazolidin-2-one → (+)-MBDB (103882-54-8,103818-46-8)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; for 5h; Ambient temperature;

DOI:10.1002/chem.19970030825

Reference yield:

(R)-1-Benzo[1,3]dioxol-5-yl-2-methylamino-butan-1-ol → (+)-MBDB (103882-54-8,103818-46-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / Et₃N / CH₂Cl₂; toluene / 1 h / Ambient temperature

2: Et₃N, H₂ / 10percent Pd/C / ethanol / 5 h / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; toluene;

DOI:10.1002/chem.19970030825