C₁₃H₁₈Se

Base Information

Chemical Name:C₁₃H₁₈Se
CAS No.:1447728-67-7
Molecular Formula:C₁₃H₁₈Se
Molecular Weight:253.246
Hs Code.:

Synonyms:

Suppliers and Price of C₁₃H₁₈Se

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₈Se

Chemical Property:

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Technology Process of C₁₃H₁₈Se

There total 1 articles about C₁₃H₁₈Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 766-00-7
2-cyclopentyl-ethanol

: 1447728-67-7
C₁₃H₁₈Se

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 3 h / Inert atmosphere

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: 1447728-67-7
C₁₃H₁₈Se

: C₁₃H₁₈OSe

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: 1447728-67-7
C₁₃H₁₈Se

: 1447729-04-5
C₁₄H₁₇BrO₂Zn

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere

3: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

4: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

With sodium benzoate; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; lithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114