(Z)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol

Base Information

Chemical Name:(Z)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol
CAS No.:76042-44-9
Molecular Formula:C₁₄H₂₄O
Molecular Weight:208.344
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol

Chemical Property:

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Technology Process of (Z)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol

There total 18 articles about (Z)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 76042-34-7
2-(2-n-butylcyclohexen-1-yl)cyclobutanone

: 76042-44-9,76042-45-0
(E)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol

Guidance literature:: With aluminum isopropoxide; In isopropyl alcohol; Heating;
DOI:10.1021/ja00547a015

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 76042-44-9,76042-45-0
(E)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / lithium diisopropylamide / tetrahydrofuran / -78 °C

2: 1.) phosphorus oxychloride, HMPA, 2.) pyridine / 1.) room temperature -> 50 deg C, 2.) 50 deg C -> 100 deg C

3: 66 percent / diethyl ether / Ambient temperature

4: 48 percent / 48percent fluoboric acid / diethyl ether

5: 78 percent / aluminium isopropoxide / propan-2-ol / Heating

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrafluoroboric acid; aluminum isopropoxide; lithium diisopropyl amide; trichlorophosphate; In tetrahydrofuran; diethyl ether; isopropyl alcohol;
DOI:10.1021/ja00547a015

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 76042-44-9,76042-45-0
(Z)-2-(2-n-butylcyclohexen-1-yl)cyclobutanol

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / lithium diisopropylamide / tetrahydrofuran / -78 °C

2: 1.) phosphorus oxychloride, HMPA, 2.) pyridine / 1.) room temperature -> 50 deg C, 2.) 50 deg C -> 100 deg C

3: 66 percent / diethyl ether / Ambient temperature

4: 48 percent / 48percent fluoboric acid / diethyl ether

5: 1.) K-Selectride, 2.) 30percent aq. hydrogen peroxide, 20percent aq. sodium hydroxide

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; tetrafluoroboric acid; dihydrogen peroxide; potassium tri-sec-butyl-borohydride; lithium diisopropyl amide; trichlorophosphate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00547a015