C₁₆H₁₄Br₄Se

Base Information

• Chemical Name: C₁₆H₁₄Br₄Se
• CAS No.: 151782-30-8
• Molecular Formula: C₁₆H₁₄Br₄Se
• Molecular Weight: 604.863
• Mol file: 151782-30-8.mol

Synonyms:

Chemical Property of C₁₆H₁₄Br₄Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₄Br₄Se

There total 2 articles about C₁₆H₁₄Br₄Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

di-2,6-dimethylphenyl selenide (151782-29-5) → C16H14Br4Se (151782-30-8)

Guidance literature:

With N-Bromosuccinimide; In tetrachloromethane; for 24h; Irradiation;

DOI:10.1016/0040-4020(96)00857-5

Reference yield:

2,6-dimethylaniline (87-62-7) → C16H14Br4Se (151782-30-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) 6N HCl, 2.) aq. NaNO₂, 3.) K₂Se

2: 21 percent / N-bromosuccinimide / CCl₄ / 24 h / Irradiation

With hydrogenchloride; N-Bromosuccinimide; potassium selenide; sodium nitrite; In tetrachloromethane;

DOI:10.1016/0040-4020(96)00857-5

Reference yield: 66.0%

benzylamine (100-46-9) + C16H14Br4Se (151782-30-8) → C30H28N2Se (151782-22-8)

Guidance literature:

In dichloromethane; for 12h; Ambient temperature;

DOI:10.1016/0040-4020(96)00857-5

upstream raw materials:

di-2,6-dimethylphenyl selenide

2,6-dimethylaniline

Downstream raw materials:

C₃₀H₂₈N₂Se

C₂₃H₂₂N₂Se