Technology Process of 3,5,3',5'-Tetraacetoxydiphenylethan
There total 5 articles about 3,5,3',5'-Tetraacetoxydiphenylethan which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 68 percent / Na / diethyl ether / 20 h / Heating
2: 81 percent / pyridine hydrochloride / 2 h / 210 °C
3: CH3COONa
With
sodium acetate; pyridine hydrochloride; sodium;
In
diethyl ether;
DOI:10.1002/ardp.19813141205
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 36 percent / potassium tert-butoxide / benzene / 1.) room temp., 20 h, 2.) 60 deg C, 1 h
2: H2 / 10percent Pd/C / ethanol
3: 81 percent / pyridine hydrochloride / 2 h / 210 °C
4: CH3COONa
With
potassium tert-butylate; hydrogen; sodium acetate; pyridine hydrochloride;
palladium on activated charcoal;
In
ethanol; benzene;
DOI:10.1002/ardp.19813141205
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2 / 10percent Pd/C / ethanol
2: 81 percent / pyridine hydrochloride / 2 h / 210 °C
3: CH3COONa
With
hydrogen; sodium acetate; pyridine hydrochloride;
palladium on activated charcoal;
In
ethanol;
DOI:10.1002/ardp.19813141205