C₆₂H₈₃N₅O₁₁S

Base Information

Chemical Name:C₆₂H₈₃N₅O₁₁S
CAS No.:1333536-78-9
Molecular Formula:C₆₂H₈₃N₅O₁₁S
Molecular Weight:1106.43
Hs Code.:

C<sub>62</sub>H<sub>83</sub>N<sub>5</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₆₂H₈₃N₅O₁₁S

Chemical Property:

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Technology Process of C₆₂H₈₃N₅O₁₁S

There total 19 articles about C₆₂H₈₃N₅O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 878626-68-7
pyrrolidine-1,2-dicarboxylic acid (2S)-2-{(1S,3S,5S,6S)-6-[5-[(1E)-2-carbonyl-1-propenyl]-(S)-4,5-dihydrothiazol-2-yl]-1-tert-butyl-5-hydroxy-3-methylhept-1-yl}ester 1-(9H-fluoren-9-ylmethyl)ester

: 1333536-74-5
C₂₃H₃₅N₃O₅

: 1333536-78-9
C₆₂H₈₃N₅O₁₁S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 20 ℃; for 10h;
DOI:10.1021/ml200176m

Reference yield:

: (S,E)-4-((tert-butoxycarbonyl)amino)-2-methyl-5-(tritylthio)pent-2-enoic acid

: 1333536-78-9
C₆₂H₈₃N₅O₁₁S

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / dimethyl sulfoxide / 20 °C

2: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 20 °C / Inert atmosphere

3: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

4: trifluoromethylsulfonic anhydride; Triphenylphosphine oxide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5: ammonium acetate; zinc / tetrahydrofuran; water / 0.5 h / 20 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylaniline / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Darkness

7: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 10 h / 20 °C

With 2,6-dimethylpyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; trifluoromethylsulfonic anhydride; trimethylsilyl trifluoromethanesulfonate; ammonium acetate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; N-methylaniline; Triphenylphosphine oxide; zinc; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ml200176m

Reference yield:

: (E)-(S)-4-Amino-2-methyl-5-tritylsulfanyl-pent-2-enoic acid allyl ester

: 1333536-78-9
C₆₂H₈₃N₅O₁₁S

Guidance literature:: Multi-step reaction with 5 steps

1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

2: trifluoromethylsulfonic anhydride; Triphenylphosphine oxide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: ammonium acetate; zinc / tetrahydrofuran; water / 0.5 h / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylaniline / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Darkness

5: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 10 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; trifluoromethylsulfonic anhydride; ammonium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; N-methylaniline; Triphenylphosphine oxide; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ml200176m