C₁₈H₁₇NO₃

Base Information

Chemical Name:C₁₈H₁₇NO₃
CAS No.:1620077-26-0
Molecular Formula:C₁₈H₁₇NO₃
Molecular Weight:295.338
Hs Code.:

C<sub>18</sub>H<sub>17</sub>NO<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₇NO₃

Chemical Property:

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Technology Process of C₁₈H₁₇NO₃

There total 3 articles about C₁₈H₁₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-38-7
para-bromotoluene

: 1620077-26-0
C₁₈H₁₇NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium; iodine / tetrahydrofuran / 3.5 h / Inert atmosphere; Reflux

1.2: 4 h / 20 °C / Inert atmosphere

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C

3.1: sodium hydroxide; hydroxylamine hydrochloride / ethanol / 6 h / Reflux

With hydroxylamine hydrochloride; iodine; magnesium; sodium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethanol; dimethyl sulfoxide;
DOI:10.1039/c4ob00744a

Reference yield:

: 1620077-14-6
(3-methoxyl-4-propargyl phenyl)(4-methylphenyl)methanol

: 1620077-26-0
C₁₈H₁₇NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C

2: sodium hydroxide; hydroxylamine hydrochloride / ethanol / 6 h / Reflux

With hydroxylamine hydrochloride; sodium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethanol; dimethyl sulfoxide;
DOI:10.1039/c4ob00744a