17β-acetoxy-28-norlupane

Base Information

• Chemical Name: 17β-acetoxy-28-norlupane
• CAS No.: 181299-08-1
• Molecular Formula: C₃₁H₅₂O₂
• Molecular Weight: 456.753

Synonyms:

Chemical Property of 17β-acetoxy-28-norlupane

Chemical Property:

Purity/Quality:

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Technology Process of 17β-acetoxy-28-norlupane

There total 3 articles about 17β-acetoxy-28-norlupane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

28-lupanol (53802-55-4) → 28-norlup-16-ene (53767-47-8) + 28-norlup-17(22)-ene (53767-52-5) + 28-norlup-17-ene (25613-22-3) + 17β-acetoxy-28-norlupane (181299-08-1)

Guidance literature:

With lead(IV) acetate; In cyclohexane; for 3h; Further byproducts given; Heating;

Reference yield:

28-lupanol (53802-55-4) → 28-norlup-17(22)-ene (53767-52-5) + 13β,28-epoxylupane (53767-44-5) + 28-norlup-17-ene (25613-22-3) + 17β-acetoxy-28-norlupane (181299-08-1)

Guidance literature:

With lead(IV) acetate; In cyclohexane; for 3h; Further byproducts given; Heating;

Reference yield:

lead(IV) tetraacetate (546-67-8) + 28-lupanol (53802-55-4) → 28-norlup-16-ene (53767-47-8) + 13β,28-epoxylupane (53767-44-5) + 28-norlup-17-ene (25613-22-3) + 17β-acetoxy-28-norlupane (181299-08-1)

Guidance literature:

In cyclohexane; for 3h; Further byproducts given; Heating;

upstream raw materials:

lead(IV) tetraacetate

28-lupanol

Downstream raw materials:

28-norlup-16-ene

28-norlup-17(22)-ene

28-norlup-17-ene

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