1,1-diacetoxy-2,6-diphenyl-4-p-nitrophenyl-1,2,3,5,6-boratetrazine

Base Information

• Chemical Name: 1,1-diacetoxy-2,6-diphenyl-4-p-nitrophenyl-1,2,3,5,6-boratetrazine
• CAS No.: 74121-72-5
• Molecular Formula: C₂₃H₂₀BN₅O₆
• Molecular Weight: 473.253
• Mol file: 74121-72-5.mol

Synonyms:

Chemical Property of 1,1-diacetoxy-2,6-diphenyl-4-p-nitrophenyl-1,2,3,5,6-boratetrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-diacetoxy-2,6-diphenyl-4-p-nitrophenyl-1,2,3,5,6-boratetrazine

There total 2 articles about 1,1-diacetoxy-2,6-diphenyl-4-p-nitrophenyl-1,2,3,5,6-boratetrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

acetic anhydride (108-24-7) + 3-(4-nitrophenyl)-1,5-diphenylformazan (6165-65-7) → 1,1-diacetoxy-2,6-diphenyl-4-p-nitrophenyl-1,2,3,5,6-boratetrazine (74121-72-5)

Guidance literature:

With boric acid; In acetic acid;

Reference yield: 45.0%

HN4C(C6H5)2(C6H4NO2) (6165-65-7,56156-44-6) + boric acid (11113-50-1,14635-83-7) → 1,1-diacetoxy-2,6-diphenyl-4-p-nitrophenyl-1,2,3,5,6-boratetrazine (74121-72-5)

Guidance literature:

With acetic anhydride; In acetic anhydride; acetic acid; heating of B(OH)3 in acetic acid anhydride and acetic acid (60°C), addn. of warm soln. of org. compd. in acetic acid anhydride and acetic acid (60°C), heating (120°C, 6 h); cooling, pouring onto ice (overnight), filtration, washing (H2O), drying (P2O5), recrystn. (benzene); elem. anal.;

upstream raw materials:

acetic anhydride

3-(4-nitrophenyl)-1,5-diphenylformazan

HN₄C(C₆H₅)2(C₆H₄NO₂)

boric acid

Refernces