N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan

Base Information

Chemical Name:N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan
CAS No.:31058-74-9
Molecular Formula:C₁₅H₁₂Cl₂N₄O
Molecular Weight:335.192
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan

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Technology Process of N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan

There total 1 articles about N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31058-74-9
N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan

Guidance literature:: Diazoniumsalz d. p-Chloranilins, Acetessigsaeure (aus Acetessigester m. verd. wss. KOH) <0grad>;

Reference yield:

: copper(II) choride dihydrate

: 31058-74-9
N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan

: Cu⁽¹⁺⁾*C₆H₄ClNNC(COCH₃)NNC₆H₄Cl^(1-)={Cu(C₆H₄ClNNC(COCH₃)NNC₆H₄Cl)}

Guidance literature:: With sodium acetate; In ethanol; addn. of CuCl2*2H2O in a small amt. of ethanol and sodium acetate to a hot soln. of C15H12Cl2N4O in ethanol; heating in water-bath for 1 h; standing for about 12 h;; ppt.; washing with hot H2O and very dild. aq. acetic acid; boiling with ethanol; drying in vac. at 110°C;;

Reference yield:

: copper(l) chloride

: 31058-74-9
N.N'-Bis-<4-chlor-phenyl>-C-acetyl-formazan

: Cu⁽¹⁺⁾*C₆H₄ClNNC(COCH₃)NNC₆H₄Cl^(1-)={Cu(C₆H₄ClNNC(COCH₃)NNC₆H₄Cl)}

Guidance literature:: With sodium acetate; In ethanol; CuCl, C15H12Cl2N4O and sodium acetate in hot ethanol;; extraction with CHCl3 or benzene;;