Technology Process of C53H80N4O6
There total 10 articles about C53H80N4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / CH2Cl2 / Ambient temperature
2: 1.) (COCl)2, DMSO, 2.) i-Pr2NEt / 1.) CH2Cl2, -78 deg C, 2.) -78 deg C to r.t.
3: 1.) Me3P, MS 4A, 2.) NaBH4 / 1.) THF, 2.) EtOH, diglyme
With
sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; trimethylphosphane;
In
dichloromethane;
DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 81 percent / NaI, K2CO3 / dimethylformamide / 48 h / Ambient temperature
2: 93 percent / Et3N, DMAP / CH2Cl2 / 5 h / Ambient temperature
3: 88 percent / Et3N / CH2Cl2 / 4 h / Ambient temperature
4: 90 percent / TBAF / tetrahydrofuran
5: Et3N / CH2Cl2 / Ambient temperature
6: NaN3, NaI / dimethylformamide
7: 1.) Me3P, MS 4A, 2.) NaBH4 / 1.) THF, 2.) EtOH, diglyme
With
dmap; sodium tetrahydroborate; sodium azide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; sodium iodide; trimethylphosphane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 88 percent / Et3N / CH2Cl2 / 4 h / Ambient temperature
2: 90 percent / TBAF / tetrahydrofuran
3: Et3N / CH2Cl2 / Ambient temperature
4: NaN3, NaI / dimethylformamide
5: 1.) Me3P, MS 4A, 2.) NaBH4 / 1.) THF, 2.) EtOH, diglyme
With
sodium tetrahydroborate; sodium azide; tetrabutyl ammonium fluoride; triethylamine; sodium iodide; trimethylphosphane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2