(+)-5-amino-3-phenylisoxazole*(+)-tartrate

Base Information

Chemical Name:(+)-5-amino-3-phenylisoxazole*(+)-tartrate
CAS No.:103772-89-0
Molecular Formula:C₄H₆O₆*C₂₄H₂₉N₃O
Molecular Weight:525.602
Hs Code.:

(+)-5-<N-benzyl-N-(1-methyl-3-pyrrolidinopropyl)>amino-3-phenylisoxazole*(+)-tartrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-5-amino-3-phenylisoxazole*(+)-tartrate

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Technology Process of (+)-5-amino-3-phenylisoxazole*(+)-tartrate

There total 5 articles about (+)-5-amino-3-phenylisoxazole*(+)-tartrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4369-55-5
3-phenyl-isoxazol-5-ylamine

: 103772-89-0,103785-28-0
(+)-5-amino-3-phenylisoxazole*(+)-tartrate

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / NaNH₂/benzene / 16 h / Heating

2: 79 percent / 70percent sodium bis-(2-methoxyethoxy)aluminum hydride in toluene / benzene / 12 h / Ambient temperature

3: 41 percent / 1) NaNH₂/benzene / 1) reflux 1.5 h 2) 50 deg C, 12 h

4: 34.8 percent / ethanol

With sodium amide; sodium bis(2-methoxyethoxy)aluminium dihydride; benzene; In ethanol; benzene;
DOI:10.1248/cpb.34.1634

Reference yield:

: 86684-32-4
(1-Methyl-3-pyrrolidin-1-yl-propyl)-(3-phenyl-isoxazol-5-yl)-amine

: 103772-89-0,103785-28-0
(+)-5-amino-3-phenylisoxazole*(+)-tartrate

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / 1) NaNH₂/benzene / 1) reflux 1.5 h 2) 50 deg C, 12 h

2: 34.8 percent / ethanol

With sodium amide; benzene; In ethanol;
DOI:10.1248/cpb.34.1634

Reference yield:

: 86684-03-9
N-<3-(3-phenyl-5-isoxaolyl)aminobutanoyl>pyrrolidine

: 103772-89-0,103785-28-0
(+)-5-amino-3-phenylisoxazole*(+)-tartrate

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / 70percent sodium bis-(2-methoxyethoxy)aluminum hydride in toluene / benzene / 12 h / Ambient temperature

2: 41 percent / 1) NaNH₂/benzene / 1) reflux 1.5 h 2) 50 deg C, 12 h

3: 34.8 percent / ethanol

With sodium amide; sodium bis(2-methoxyethoxy)aluminium dihydride; benzene; In ethanol; benzene;
DOI:10.1248/cpb.34.1634