dimethyl(phenylaminomethyl)vinylgermane

Base Information

Chemical Name:dimethyl(phenylaminomethyl)vinylgermane
CAS No.:118165-94-9
Molecular Formula:C₁₁H₁₇GeN
Molecular Weight:235.853
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl(phenylaminomethyl)vinylgermane

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Technology Process of dimethyl(phenylaminomethyl)vinylgermane

There total 1 articles about dimethyl(phenylaminomethyl)vinylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 118165-93-8
chloromethyldimethylvinylgermane

: 118165-94-9
dimethyl(phenylaminomethyl)vinylgermane

Guidance literature:: With aniline; In dimethyl sulfoxide; under N2; mixt. of germane and amine was heated at 80 ° C for 10 h;; mixt. was mixed with water, extn. with ether; extract dried, concn., distn., elem. anal.;
DOI:10.1016/S0022-328X(00)99387-2

Reference yield: 56.0%

: 118165-94-9
dimethyl(phenylaminomethyl)vinylgermane

: 118165-95-0
3,3-dimethyl-1-phenyl-1,3-azagermolidine

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate; In tetrahydrofuran; water; under N2; to stirring mixt. of Hg(OAc)2 (1.11 mmol),THF, H2O was added germane (1.11 mmol) at room temp., after 4 h 0.5 N NaOH was added, followed by soln. of NaBH4 (1.16 mmol) in 2.5 N NaOH, stirring for 2 h;; mixt. filtered,extn. (ether),residue of ether extract mixed with acetic anhydride to separate it from starting germane;stirring for 2 h,mixt. added to 5% HCl, extn. (ether),neutralized with aq. NaOH, extn. (ether),concn.,distn.,elem. anal.;
DOI:10.1016/S0022-328X(00)99387-2