diphenyllead bis(4-methylbenzenecarboselenoate)

Base Information

Chemical Name:diphenyllead bis(4-methylbenzenecarboselenoate)
CAS No.:128816-58-0
Molecular Formula:C₂₈H₂₄O₂PbSe₂
Molecular Weight:757.617
Hs Code.:

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Chemical Property of diphenyllead bis(4-methylbenzenecarboselenoate)

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Technology Process of diphenyllead bis(4-methylbenzenecarboselenoate)

There total 1 articles about diphenyllead bis(4-methylbenzenecarboselenoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2117-69-3
diphenyllead(IV) dichloride

: potassium 4-methylbenzenecarboselenoate

: 128816-58-0
diphenyllead bis(4-methylbenzenecarboselenoate)

Guidance literature:: In diethyl ether; byproducts: KCl; addn. of Ph2PbCl2 to a suspn. of K-selenocarboxylate in ether, stirring at 20°C for 1 h (under Ar); filtn. of KCl-ppt., evapn. of the solvent in vacuo, recrystn. from ether/hexane, elem. anal.;
DOI:10.1016/0022-328X(90)80004-J

Reference yield: 60.0%

: 34837-55-3
Phenylselenyl bromide

: 128816-58-0
diphenyllead bis(4-methylbenzenecarboselenoate)

: 111931-77-2
Se(Se)-phenyl 4-methyl(diseleno)perbenzoate

Guidance literature:: In diethyl ether; at 20 ℃; for 1h;
DOI:10.1016/0022-328X(90)80004-J

Reference yield: 60.0%

: 128816-58-0
diphenyllead bis(4-methylbenzenecarboselenoate)

: 34837-55-3
Phenylselenyl bromide

: 111931-77-2
Se(Se)-phenyl 4-methyl(diseleno)perbenzoate

Guidance literature:: In diethyl ether; byproducts: (C6H5)2PbBr2; addn. of PhSeBr to a soln. of (MePhCOSe)2PbPh2 in ether, stirring at 20°C for 1 h (under Ar); concn., addn. of hexane, cooling to -20°C for 5 h, filtn.;
DOI:10.1016/0022-328X(90)80004-J