1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate

Base Information

Chemical Name:1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate
CAS No.:1453496-20-2
Molecular Formula:C₁₆H₁₃NO₅
Molecular Weight:300.275
Hs Code.:

1-oxo-3-phenyl(1-<SUP>2</SUP>H)propan-2-yl 4-nitrobenzoate

Synonyms:

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Chemical Property of 1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate

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Technology Process of 1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate

There total 2 articles about 1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-25-3
3-phenylpropanoic acid methyl ester

: 1453496-20-2
1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium deuteride / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 3 h / 0 - 20 °C

3: tetra-(n-butyl)ammonium iodide; piperidine; tert.-butylhydroperoxide / decane; ethyl acetate / 5 h / 50 °C

With piperidine; tert.-butylhydroperoxide; lithium aluminium deuteride; sulfur trioxide pyridine complex; tetra-(n-butyl)ammonium iodide; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; decane; dichloromethane; ethyl acetate;
DOI:10.1021/jo401433q

Reference yield:

: 17428-96-5
1,1-d2-3-phenylpropan-1-ol

: 1453496-20-2
1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 3 h / 0 - 20 °C

2: tetra-(n-butyl)ammonium iodide; piperidine; tert.-butylhydroperoxide / decane; ethyl acetate / 5 h / 50 °C

With piperidine; tert.-butylhydroperoxide; sulfur trioxide pyridine complex; tetra-(n-butyl)ammonium iodide; dimethyl sulfoxide; triethylamine; In decane; dichloromethane; ethyl acetate;
DOI:10.1021/jo401433q

Reference yield:

: 1184844-25-4
(E)-4,4,4-trifluoro-1-(4-methoxyphenyl)-2-buten-1-one

: 1453496-20-2
1-oxo-3-phenyl(1-²H)propan-2-yl 4-nitrobenzoate

: 1453496-06-4
C₂₀H₁₇F₃O₃

Guidance literature:: With (5aR,10bS)-5a,10b-dihydro-2-(2,4,6-trimethylphenyl)-4H,6H-indeno[2,1-b]-1,2,4-triazolo[4,3-d]-1,4-oxazinium chloride; triethylamine; In dichloromethane-d2; at 20 ℃; stereospecific reaction; Kinetics;
DOI:10.1021/jo401433q