GSK 2200150A

Base Information

Chemical Name:GSK 2200150A
CAS No.:1443138-53-1
Molecular Formula:C₂₀H₂₃NO₃S
Molecular Weight:357.474
Hs Code.:

Synonyms:

Suppliers and Price of GSK 2200150A

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

DC Chemicals
GSK-2200150A >98%
250 mg
$ 1100.00

ChemScene
GSK2200150A 98.46%
50mg
$ 240.00

ChemScene
GSK2200150A 98.46%
25mg
$ 150.00

ChemScene
GSK2200150A 98.46%
10mg
$ 80.00

ChemScene
GSK2200150A 98.46%
5mg
$ 50.00

Total 10 raw suppliers

Chemical Property of GSK 2200150A

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

GSK-2200150A >98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of GSK 2200150A

There total 6 articles about GSK 2200150A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 6',7'-dihydrospiro[piperidine-4,4'-thieno[3,2-c]pyran]

: 29668-44-8
2,3-dihydro-benzo[1,4]dioxin-6-carbaldehyde

: 1443138-53-1
GSK 2200150A

Guidance literature:: With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1371/journal.pone.0111782

Reference yield:

: 1093378-98-3
1-benzyl-6',7'-dihydrospiro[piperidine-4,4'-thieno[3,2-c]pyran]

: 1443138-53-1
GSK 2200150A

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

1.2: 1 h / Reflux

2.1: sodium hydroxide / 1,4-dioxane; water / 4 h / Reflux

3.1: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1371/journal.pone.0111782

Reference yield:

: 5402-55-1
2-thiophenethanol

: 1443138-53-1
GSK 2200150A

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanesulfonic acid / toluene / 16 h / 130 °C

2.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.2: 1 h / Reflux

3.1: sodium hydroxide / 1,4-dioxane; water / 4 h / Reflux

4.1: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C / Inert atmosphere

With methanesulfonic acid; sodium tris(acetoxy)borohydride; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; 1.1: |Pictet-Spengler Synthesis;
DOI:10.1371/journal.pone.0111782