C₂₀H₂₉ClN₂O₈

Base Information

Chemical Name:C₂₀H₂₉ClN₂O₈
CAS No.:1027604-35-8
Molecular Formula:C₂₀H₂₉ClN₂O₈
Molecular Weight:460.912
Hs Code.:

C<sub>20</sub>H<sub>29</sub>ClN<sub>2</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₂₀H₂₉ClN₂O₈

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Technology Process of C₂₀H₂₉ClN₂O₈

There total 8 articles about C₂₀H₂₉ClN₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 184841-34-7
C₂₇H₃₅ClN₂O₈

: 1027604-35-8
C₂₀H₂₉ClN₂O₈

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/0040-4039(96)01829-1

Reference yield:

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 1027604-35-8
C₂₀H₂₉ClN₂O₈

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MeZnBr; 2. ) LDA; 3.) NH₄Cl / 1.) 0 deg C; 2.) -78 deg C; 3.) H₂O, -78 deg C

2: hydrogen / Pd/C / methanol

With hydrogen; ammonium chloride; lithium diisopropyl amide; zinc methyl bromide; palladium on activated charcoal; In methanol;
DOI:10.1016/0040-4039(96)01829-1

Reference yield:

: 3964-58-7
3-chloro-4-hydroxybenzoic acid

: 1027604-35-8
C₂₀H₂₉ClN₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1: dimethylformamide

2: 2N NaOH / methanol

3: SOCl₂

4: MgCl₂, Et₃N / acetonitrile

5: 100 percent / hydrogen, RuBr₂<(R)-Binap> / CH₂Cl₂ / 27 °C / 4500.4 Torr

6: 1.) MeZnBr; 2. ) LDA; 3.) NH₄Cl / 1.) 0 deg C; 2.) -78 deg C; 3.) H₂O, -78 deg C

7: hydrogen / Pd/C / methanol

With sodium hydroxide; thionyl chloride; [(R)-BINAP]RuBr₂; hydrogen; ammonium chloride; triethylamine; magnesium chloride; lithium diisopropyl amide; zinc methyl bromide; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(96)01829-1