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C5H4BBr2FeC5H4BBrNSi(CH3)3BrC6H4

Base Information
  • Chemical Name:C5H4BBr2FeC5H4BBrNSi(CH3)3BrC6H4
  • CAS No.:507229-50-7
  • Molecular Formula:C19H21B2Br4FeNSi
  • Molecular Weight:688.553
  • Hs Code.:
C<sub>5</sub>H<sub>4</sub>BBr<sub>2</sub>FeC<sub>5</sub>H<sub>4</sub>BBrNSi(CH<sub>3</sub>)3BrC<sub>6</sub>H<sub>4</sub>

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Suppliers and Price of C5H4BBr2FeC5H4BBrNSi(CH3)3BrC6H4
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C5H4BBr2FeC5H4BBrNSi(CH3)3BrC6H4
Chemical Property:
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Technology Process of C5H4BBr2FeC5H4BBrNSi(CH3)3BrC6H4

There total 1 articles about C5H4BBr2FeC5H4BBrNSi(CH3)3BrC6H4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In toluene; ligand in toluene was added with stirring to Fe-complex in toluene at -78°C, warmed to ambient temp., stirred for 4 h under Ar; evapd. in vacuo, triturated with C6H14;
DOI:10.1016/S0022-328X(02)01968-X
Guidance literature:
In toluene; Fe-complex in toluene was refluxed for 2.5 h under Ar; concd., stored at -30°C overnight, filtered, concd., crystd. uponstorage at -30°C for 12 h, filtered, triturated with C5H12, drie d in vacuo;
DOI:10.1016/S0022-328X(02)01968-X
upstream raw materials:

2-(4-bromophenyl)-1,1,1,3,3,3-hexamethyldisilazane

Downstream raw materials:

1,3-dibora-[3]ferrocenophane

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