nitrosyltetrakis(2,4,6-trimethylthiophenolato)rhenium

Base Information

Chemical Name:nitrosyltetrakis(2,4,6-trimethylthiophenolato)rhenium
CAS No.:99083-41-7
Molecular Formula:C₃₆H₄₄NOReS₄
Molecular Weight:821.222
Hs Code.:

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Chemical Property of nitrosyltetrakis(2,4,6-trimethylthiophenolato)rhenium

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Technology Process of nitrosyltetrakis(2,4,6-trimethylthiophenolato)rhenium

There total 1 articles about nitrosyltetrakis(2,4,6-trimethylthiophenolato)rhenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1541-10-2
mesitylthiol

: 83095-49-2
bis(triphenylphosphane)methoxydichloronitrosylrhenium

: 99083-41-7
nitrosyltetrakis(2,4,6-trimethylthiophenolato)rhenium

Guidance literature:: With (C₂H₅)3N; In methanol; to a stirred suspn. of Re-compd. (0.24 mmol) in MeOH were added (under N2) HSC6H2Me3-2,4,6 (1.18 mmol) and (C2H5)3N (1.16 mmol); the mixt. was heated under reflux for 0.5 h;; hot soln. was filtered; crystn. from filtrate on cooling; the insol. residue was extd. with diethyl ether, the resulting soln. was filtered andevapd. to dryness; recrystn. from hot methanol; elem. anal.;;

Reference yield:

: 99083-41-7
nitrosyltetrakis(2,4,6-trimethylthiophenolato)rhenium

: 99101-84-5
methoxonitrosyltris(2,4,6-trimethylthiophenolato)rhenium

Guidance literature:: With CH₃OH; In methanol; dichloromethane; CH2Cl2-MeOH soln. of Re-compd. at room temp. for several days under N2;; partial evapn.; elem. anal.;;