Technology Process of C17H20O2Se
There total 6 articles about C17H20O2Se which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
1.) -78 deg C, 1h, 2.) -20 deg C, 15 min;
DOI:10.1016/S0040-4039(01)92929-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / K2CO3 / dimethylformamide / 0.5 h / 25 °C
2: 97 percent / NaH / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.) 25 deg C, 2 h 2.) reflux 16 h
3: m-ClPBA / CH2Cl2 / 1.) -78 deg C, 1h, 2.) -20 deg C, 15 min
With
sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)92929-6
- Guidance literature:
-
Multi-step reaction with 5 steps
2: 93 percent / t-BuOK / 2-methyl-propan-2-ol; diethyl ether / 0.33 h / 25 °C
3: 90 percent / K2CO3 / dimethylformamide / 0.5 h / 25 °C
4: 97 percent / NaH / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.) 25 deg C, 2 h 2.) reflux 16 h
5: m-ClPBA / CH2Cl2 / 1.) -78 deg C, 1h, 2.) -20 deg C, 15 min
With
potassium tert-butylate; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/S0040-4039(01)92929-6
