C₂₃H₂₃N₃O₅S

Base Information

Chemical Name:C₂₃H₂₃N₃O₅S
CAS No.:121711-36-2
Molecular Formula:C₂₃H₂₃N₃O₅S
Molecular Weight:453.519
Hs Code.:

C<sub>23</sub>H<sub>23</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₃H₂₃N₃O₅S

Chemical Property:

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Technology Process of C₂₃H₂₃N₃O₅S

There total 9 articles about C₂₃H₂₃N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 73034-19-2,74645-66-2
(+/-)-γ-lycoran-3-one lactam

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 121711-36-2
C₂₃H₂₃N₃O₅S

Guidance literature:: In methanol; for 2h; Heating;

Reference yield:

: 65628-88-8
2-benzylhomophthalimide

: 121711-36-2
C₂₃H₂₃N₃O₅S

Guidance literature:: Multi-step reaction with 9 steps

1: 65 percent / Triton-B / acetone; H₂O / 0.5 h / Ambient temperature

2: p-toluenesulfonic acid / benzene / 3 h / Heating; azeotrope distillation

3: NaBH₄ / methanol / 1 h / Ambient temperature

4: 90 percent / p-toluenesulfonic acid / benzene / Heating; azeotrope distillation

5: 1) LiAlH₄ 2) 12N aq. HCl / 1) tetrahydrofuran, ice cooling 2) 100 deg. C, 1 h

6: 90 percent / H₂ / PdCl₂ / methanol; aq. HCl / 4 h / 760 Torr / Ambient temperature

7: 95 percent / triethylamine / CH₂Cl₂ / 1 h / Ambient temperature

8: 85 percent / potassium t-butoxide / 2-methyl-propan-2-ol / 0.5 h / Heating

9: 85 percent / methanol / 2 h / Heating

With hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; potassium tert-butylate; hydrogen; N-benzyl-trimethylammonium hydroxide; toluene-4-sulfonic acid; triethylamine; palladium dichloride; In hydrogenchloride; methanol; dichloromethane; water; acetone; tert-butyl alcohol; benzene;

Reference yield:

: 121696-00-2
2-benzyl-6,7-methylenedioxy-4-(3-oxobutyl)isocarbostyril

: 121711-36-2
C₂₃H₂₃N₃O₅S

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / p-toluenesulfonic acid / benzene / Heating; azeotrope distillation

2: 1) LiAlH₄ 2) 12N aq. HCl / 1) tetrahydrofuran, ice cooling 2) 100 deg. C, 1 h

3: 90 percent / H₂ / PdCl₂ / methanol; aq. HCl / 4 h / 760 Torr / Ambient temperature

4: 95 percent / triethylamine / CH₂Cl₂ / 1 h / Ambient temperature

5: 85 percent / potassium t-butoxide / 2-methyl-propan-2-ol / 0.5 h / Heating

6: 85 percent / methanol / 2 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; potassium tert-butylate; hydrogen; toluene-4-sulfonic acid; triethylamine; palladium dichloride; In hydrogenchloride; methanol; dichloromethane; tert-butyl alcohol; benzene;