(+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide

Base Information

• Chemical Name: (+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide
• CAS No.: 111502-22-8
• Molecular Formula: C₁₉H₁₅Cl₇S
• Molecular Weight: 523.565
• Mol file: 111502-22-8.mol

Synonyms:

Chemical Property of (+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide

There total 2 articles about (+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methylbenzenesulfenyl chloride (933-00-6) → (+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide (111502-22-8)

Guidance literature:

With tetrachloromethane;

DOI:10.1021/ja01579a051

Reference yield:

para-thiocresol (106-45-6) → (+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide (111502-22-8)

Guidance literature:

With hexane;

DOI:10.1021/ja01579a052

Reference yield:

(+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfide (111502-22-8) → (+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfone (101894-95-5)

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/ja01579a051

upstream raw materials:

p-methylbenzenesulfenyl chloride

para-thiocresol

Downstream raw materials:

(+/-)-(3t,5,6,7,8,9,9-heptachloro-(4at,8at)-1,2,3,4,4a,5,8,8a-octahydro-1r,4c;5t,8t-dimethano-naphthalen-2c-yl)-p-tolyl sulfone