Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Base Information

Chemical Name:Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide
CAS No.:848827-50-9
Molecular Formula:C₇₀H₁₁₂N₂O₈
Molecular Weight:1109.67
Hs Code.:

Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Synonyms:

Suppliers and Price of Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

There total 4 articles about Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-Hexacosanoylamino-3-hydroxy-propionic acid methyl ester

: 848827-50-9
Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodosuccinimide; molecular sieves 4 Angstroem; trifluoromethanesulfonic acid / CH₂Cl₂ / -15 - -10 °C

2: sodium hydroxide / H₂O; tetrahydrofuran

3: 1-hydroxybenzotriazole hydrate / 1,2-dichloro-ethane; CH₂Cl₂

With sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: 848827-48-5
(S)-3-((2R,4aR,6S,7R,8S,8aR)-7,8-Bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hexacosanoylamino-propionic acid methyl ester

: 848827-50-9
Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / H₂O; tetrahydrofuran

2: 1-hydroxybenzotriazole hydrate / 1,2-dichloro-ethane; CH₂Cl₂

With sodium hydroxide; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: 87470-70-0
S-phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-thio-β-D-glucopyranoside

: 848827-50-9
Hexacosanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodosuccinimide; molecular sieves 4 Angstroem; trifluoromethanesulfonic acid / CH₂Cl₂ / -15 - -10 °C

2: sodium hydroxide / H₂O; tetrahydrofuran

3: 1-hydroxybenzotriazole hydrate / 1,2-dichloro-ethane; CH₂Cl₂

With sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027