C₃₇H₃₇ClN₂O₄S

Base Information

Chemical Name:C₃₇H₃₇ClN₂O₄S
CAS No.:1170704-49-0
Molecular Formula:C₃₇H₃₇ClN₂O₄S
Molecular Weight:641.231
Hs Code.:

C<sub>37</sub>H<sub>37</sub>ClN<sub>2</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₃₇H₃₇ClN₂O₄S

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Technology Process of C₃₇H₃₇ClN₂O₄S

There total 6 articles about C₃₇H₃₇ClN₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1170704-48-9
C₃₀H₃₂ClNO₄

: 103-72-0
phenyl isothiocyanate

: 1170704-49-0
C₃₇H₃₇ClN₂O₄S

Guidance literature:: With potassium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.02.038

Reference yield:

: C₂₇H₄₂O₄Si

: 1170704-49-0
C₃₇H₃₇ClN₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

3.1: cerium(III) chloride; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -70 °C / Inert atmosphere

4.1: potassium hydride / tetrahydrofuran; mineral oil / 4 h / 20 °C

With n-butyllithium; cerium(III) chloride; tetrabutyl ammonium fluoride; potassium hydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; hexane; dichloromethane; mineral oil;
DOI:10.1021/jo2002616

Reference yield:

: 1082947-06-5
C₂₁H₂₆O₄

: 1170704-49-0
C₃₇H₃₇ClN₂O₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: cerium(III) chloride; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -70 °C / Inert atmosphere

2.1: potassium hydride / tetrahydrofuran; mineral oil / 4 h / 20 °C

With n-butyllithium; cerium(III) chloride; potassium hydride; In tetrahydrofuran; hexane; mineral oil;
DOI:10.1021/jo2002616