ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate

Base Information

Chemical Name:ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate
CAS No.:98525-92-9
Molecular Formula:C₁₆H₂₁NO₃
Molecular Weight:275.348
Hs Code.:

ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopent<c>isoxazole-3-carboxylate

Synonyms:

Suppliers and Price of ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate

Chemical Property:

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Technology Process of ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate

There total 4 articles about ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98525-83-8
ethyl (Z)-7-oxo-3-phenyl-2-heptenoate

: 98525-92-9
ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / benzene / Ambient temperature

2: toluene / 12 h / Heating

With potassium carbonate; In toluene; benzene;
DOI:10.1021/jo00223a003

Reference yield:

: 98525-82-7
(Z)-ethyl 7-hydroxy-3-phenyl-2-heptenoate

: 98525-92-9
ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / oxalyl chloride, Me₂SO / CH₂Cl₂ / 0.25 h / -60 °C

2: K₂CO₃ / benzene / Ambient temperature

3: toluene / 12 h / Heating

With oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; In dichloromethane; toluene; benzene;
DOI:10.1021/jo00223a003

Reference yield:

: 98525-81-6
ethyl (Z)-7-<(tetrahydro-2H-pyran-2-yl)oxy>-3-phenylhept-2-enoate

: 98525-92-9
ethyl (3β,3aβ,6aβ)-hexahydro-1-methyl-3a-phenyl-1H-cyclopentisoxazole-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / aq. HCl / ethanol / Ambient temperature

2: 62 percent / oxalyl chloride, Me₂SO / CH₂Cl₂ / 0.25 h / -60 °C

3: K₂CO₃ / benzene / Ambient temperature

4: toluene / 12 h / Heating

With hydrogenchloride; oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; In ethanol; dichloromethane; toluene; benzene;
DOI:10.1021/jo00223a003