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Technology Process of (CH3)2CHCH2Al(N(CH3)2C6H5)OC6H2CH3(C(C6H5)3)CH2N(CH3)2(1+)*HB(C6F5)3(1-)=C4H9AlNC2H6C6H5OC6H2CH3CC18H15CH2NC2H6HBC18F15

(CH3)2CHCH2Al(N(CH3)2C6H5)OC6H2CH3(C(C6H5)3)CH2N(CH3)2(1+)*HB(C6F5)3(1-)=C4H9AlNC2H6C6H5OC6H2CH3CC18H15CH2NC2H6HBC18F15

Base Information
  • Chemical Name:(CH3)2CHCH2Al(N(CH3)2C6H5)OC6H2CH3(C(C6H5)3)CH2N(CH3)2(1+)*HB(C6F5)3(1-)=C4H9AlNC2H6C6H5OC6H2CH3CC18H15CH2NC2H6HBC18F15
  • CAS No.:777941-37-4
  • Molecular Formula:C18HBF15*C41H48AlN2O
  • Molecular Weight:1124.82
  • Hs Code.:
(CH<sub>3</sub>)2CHCH<sub>2</sub>Al(N(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)OC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>(C(C<sub>6</sub>H<sub>5</sub>)3)CH<sub>2</sub>N(CH<sub>3</sub>)2<sup>(1+)</sup>*HB(C<sub>6</sub>F<sub>5</sub>)3<sup>(1-)</sup>=C<sub>4</sub>H<sub>9</sub>AlNC<sub>2</sub>H<sub>6</sub>C<sub>6</sub>H<sub>5</sub>OC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>CC<sub>18</sub>H<sub>15</sub>CH<sub>2</sub>NC<sub>2</sub>H<sub>6</sub>HBC<sub>18</sub>F<sub>15</sub>

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Chemical Property of (CH3)2CHCH2Al(N(CH3)2C6H5)OC6H2CH3(C(C6H5)3)CH2N(CH3)2(1+)*HB(C6F5)3(1-)=C4H9AlNC2H6C6H5OC6H2CH3CC18H15CH2NC2H6HBC18F15
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Technology Process of (CH3)2CHCH2Al(N(CH3)2C6H5)OC6H2CH3(C(C6H5)3)CH2N(CH3)2(1+)*HB(C6F5)3(1-)=C4H9AlNC2H6C6H5OC6H2CH3CC18H15CH2NC2H6HBC18F15

There total 1 articles about (CH3)2CHCH2Al(N(CH3)2C6H5)OC6H2CH3(C(C6H5)3)CH2N(CH3)2(1+)*HB(C6F5)3(1-)=C4H9AlNC2H6C6H5OC6H2CH3CC18H15CH2NC2H6HBC18F15 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

((CH<sub>3</sub>)2CHCH<sub>2</sub>)2AlOC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>(C(C<sub>6</sub>H<sub>5</sub>)3)CH<sub>2</sub>N(CH<sub>3</sub>)2

((CH3)2CHCH2)2AlOC6H2CH3(C(C6H5)3)CH2N(CH3)2

tris(pentafluorophenyl)borate
1109-15-5

tris(pentafluorophenyl)borate

<i>N</i>,<i>N</i>-dimethyl-aniline
121-69-7,77733-26-7

N,N-dimethyl-aniline

(CH<sub>3</sub>)2CHCH<sub>2</sub>Al(N(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)OC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>(C(C<sub>6</sub>H<sub>5</sub>)3)CH<sub>2</sub>N(CH<sub>3</sub>)2<sup>(1+)</sup>*HB(C<sub>6</sub>F<sub>5</sub>)3<sup>(1-)</sup>=C<sub>4</sub>H<sub>9</sub>AlNC<sub>2</sub>H<sub>6</sub>C<sub>6</sub>H<sub>5</sub>OC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>CC<sub>18</sub>H<sub>15</sub>CH<sub>2</sub>NC<sub>2</sub>H<sub>6</sub>HBC<sub>18</sub>F<sub>15</sub>
777941-37-4

(CH3)2CHCH2Al(N(CH3)2C6H5)OC6H2CH3(C(C6H5)3)CH2N(CH3)2(1+)*HB(C6F5)3(1-)=C4H9AlNC2H6C6H5OC6H2CH3CC18H15CH2NC2H6HBC18F15

Guidance literature:
In dichloromethane; byproducts: isobutene; (N2); addn. of boron compd. to a soln. of aluminum complex and amine in CH2Cl2 at room temp., stirring for 1 h; evapn., trituration woth cold pentane, filtration, drying in vac.;
DOI:10.1021/om0400806
upstream raw materials:

tris(pentafluorophenyl)borate

N,N-dimethyl-aniline

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