Technology Process of C33H31ClFN3O12S
There total 11 articles about C33H31ClFN3O12S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; potassium carbonate;
In
methanol;
at 80 ℃;
DOI:10.1021/jm3014844
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C
1.2: 0.25 h / 60 °C
2.1: triphenylphosphine; di-isopropyl azodicarboxylate / dichloromethane / 0.33 h / 20 - 60 °C
3.1: zinc; ammonium chloride / water; acetone / 0.17 h / 20 °C
4.1: hydrogenchloride / methanol / 0.25 h / 60 °C
5.1: triethylamine / tetrahydrofuran / -20 °C
6.1: triethylamine / tetrahydrofuran / 0.08 h / 100 °C
7.1: potassium carbonate; water / methanol / 80 °C
With
hydrogenchloride; di-isopropyl azodicarboxylate; water; sodium hydride; potassium carbonate; ammonium chloride; triethylamine; triphenylphosphine; zinc;
In
tetrahydrofuran; methanol; dichloromethane; water; acetone; mineral oil;
DOI:10.1021/jm3014844
- Guidance literature:
-
Multi-step reaction with 5 steps
1: zinc; ammonium chloride / water; acetone / 0.17 h / 20 °C
2: hydrogenchloride / methanol / 0.25 h / 60 °C
3: triethylamine / tetrahydrofuran / -20 °C
4: triethylamine / tetrahydrofuran / 0.08 h / 100 °C
5: potassium carbonate; water / methanol / 80 °C
With
hydrogenchloride; water; potassium carbonate; ammonium chloride; triethylamine; zinc;
In
tetrahydrofuran; methanol; water; acetone;
DOI:10.1021/jm3014844
