2,6-Trip₂H₃C₆Sn-Sn(Me)2C₆H₃-2,6-Trip₂

Base Information

Chemical Name:2,6-Trip₂H₃C₆Sn-Sn(Me)2C₆H₃-2,6-Trip₂
CAS No.:317351-33-0
Molecular Formula:C₇₄H₁₀₄Sn₂
Molecular Weight:1231.06
Hs Code.:

2,6-Trip<sub>2</sub>H<sub>3</sub>C<sub>6</sub>Sn-Sn(Me)2C<sub>6</sub>H<sub>3</sub>-2,6-Trip<sub>2</sub>

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Suppliers and Price of 2,6-Trip₂H₃C₆Sn-Sn(Me)2C₆H₃-2,6-Trip₂

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Chemical Property of 2,6-Trip₂H₃C₆Sn-Sn(Me)2C₆H₃-2,6-Trip₂

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Technology Process of 2,6-Trip₂H₃C₆Sn-Sn(Me)2C₆H₃-2,6-Trip₂

There total 1 articles about 2,6-Trip₂H₃C₆Sn-Sn(Me)2C₆H₃-2,6-Trip₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 199169-92-1
Sn(Cl)(C₆H₃-2,6-(C₆H₂-2,4,6-i-Pr₃)2)

: 917-54-4
methyllithium

: 317351-33-0
2,6-Trip₂H₃C₆Sn-Sn(Me)2C₆H₃-2,6-Trip₂

Guidance literature:: In hexane; MeLi was added dropwise tosoln. ClSnC6H3-2,6-Trip2 in hexane at -78°C, soln. was stirred at -78°C for 30 min and allowed to warm to 25°C; solvent was removed under reduced pressure, residue was extd. with hexane, filtered, soln. was concd. and stored at -20°C overnight; elem. anal.;
DOI:10.1021/ic0005137