C₂₄H₃₂O₆

Base Information

Chemical Name:C₂₄H₃₂O₆
CAS No.:1430812-36-4
Molecular Formula:C₂₄H₃₂O₆
Molecular Weight:416.514
Hs Code.:

C<sub>24</sub>H<sub>32</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₂O₆

Chemical Property:

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Technology Process of C₂₄H₃₂O₆

There total 10 articles about C₂₄H₃₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1430812-35-3
C₂₄H₂₆O₆

: 1430812-36-4
C₂₄H₃₂O₆

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; acetic acid; at 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2012.12.042

Reference yield:

: 63638-85-7
3-bromo-2-hydroxy-4-methoxybenzaldehyde

: 1430812-36-4
C₂₄H₃₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1: potassium carbonate / acetonitrile / 1 h / Reflux

2: tetrahydrofuran / 1 h / 0 - 20 °C

3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 1 h / 20 °C / Inert atmosphere

4: hydrogen; palladium on activated charcoal / acetic acid; methanol / 1 h / 20 °C

5: pyridinium chlorochromate / dichloromethane / 4 h

6: toluene-4-sulfonic acid; magnesium sulfate / 2 h / Reflux

7: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; lithium tert-butoxide / 1,4-dioxane / 1 h / 90 °C

8: bis-triphenylphosphine-palladium(II) chloride; diethylamine; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 0.42 h / 120 °C / Microwave irradiation

9: hydrogen; palladium on activated charcoal / acetic acid; methanol / 3 h / 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; palladium on activated charcoal; hydrogen; magnesium sulfate; potassium carbonate; toluene-4-sulfonic acid; diethylamine; triphenylphosphine; pyridinium chlorochromate; lithium tert-butoxide; XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ejmech.2012.12.042

Reference yield:

: 1430812-44-4
1-(2-(allyloxy)-3-bromo-4-methoxyphenyl)prop-2-en-1-ol

: 1430812-36-4
C₂₄H₃₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: hydrogen; palladium on activated charcoal / acetic acid; methanol / 1 h / 20 °C

3: pyridinium chlorochromate / dichloromethane / 4 h

4: toluene-4-sulfonic acid; magnesium sulfate / 2 h / Reflux

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; lithium tert-butoxide / 1,4-dioxane / 1 h / 90 °C

6: bis-triphenylphosphine-palladium(II) chloride; diethylamine; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 0.42 h / 120 °C / Microwave irradiation

7: hydrogen; palladium on activated charcoal / acetic acid; methanol / 3 h / 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; palladium on activated charcoal; hydrogen; magnesium sulfate; toluene-4-sulfonic acid; diethylamine; triphenylphosphine; pyridinium chlorochromate; lithium tert-butoxide; XPhos; In 1,4-dioxane; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.12.042