C₂₃H₂₇ClIO₁₁P

Base Information

Chemical Name:C₂₃H₂₇ClIO₁₁P
CAS No.:219702-36-0
Molecular Formula:C₂₃H₂₇ClIO₁₁P
Molecular Weight:672.792
Hs Code.:

C<sub>23</sub>H<sub>27</sub>ClIO<sub>11</sub>P

Synonyms:

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Chemical Property of C₂₃H₂₇ClIO₁₁P

Chemical Property:

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Technology Process of C₂₃H₂₇ClIO₁₁P

There total 5 articles about C₂₃H₂₇ClIO₁₁P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131675-55-3
phenyl 2,4-di-O-acetyl-3-O-methyl-1-thio-α-L-rhamnopyranoside

: 219702-36-0
C₂₃H₂₇ClIO₁₁P

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / NIS; TMSOTf; 4 Angstroem molecular sieves / CH₂Cl₂; toluene / 2 h / 0 °C

2: 75 percent / TBAF / tetrahydrofuran / 4 h / 20 °C

3: 60 percent / RuCl₃*H₂O; NaIO₄ / CCl₄; acetonitrile; H₂O / 1 h / 20 °C

4: 79 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

5: pyridine / 1,2-dimethoxy-ethane / 1 h / 20 °C

With pyridine; ruthenium trichloride; lithium hydroxide; sodium periodate; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; tetrabutyl ammonium fluoride; dihydrogen peroxide; In tetrahydrofuran; tetrachloromethane; 1,2-dimethoxyethane; dichloromethane; water; toluene; acetonitrile; 3: Sharpless oxidation;
DOI:10.1039/b006113l

Reference yield:

: 153693-56-2
4-(tert-Butyl-diphenyl-silanyloxymethyl)-2-iodo-5,6-dimethoxy-3-methyl-phenol

: 219702-36-0
C₂₃H₂₇ClIO₁₁P

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / NIS; TMSOTf; 4 Angstroem molecular sieves / CH₂Cl₂; toluene / 2 h / 0 °C

2: 75 percent / TBAF / tetrahydrofuran / 4 h / 20 °C

3: 60 percent / RuCl₃*H₂O; NaIO₄ / CCl₄; acetonitrile; H₂O / 1 h / 20 °C

4: 79 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

5: pyridine / 1,2-dimethoxy-ethane / 1 h / 20 °C

With pyridine; ruthenium trichloride; lithium hydroxide; sodium periodate; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; tetrabutyl ammonium fluoride; dihydrogen peroxide; In tetrahydrofuran; tetrachloromethane; 1,2-dimethoxyethane; dichloromethane; water; toluene; acetonitrile; 3: Sharpless oxidation;
DOI:10.1039/b006113l

Reference yield:

: 220098-53-3
4-(2,4-Di-O-acetyl-6-deoxy-3-O-methyl-α-L-mannopyranosyloxy)-3-iodo-5,6-dimethoxy-2-methylbenzoic acid

: 219702-36-0
C₂₃H₂₇ClIO₁₁P

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

2: pyridine / 1,2-dimethoxy-ethane / 1 h / 20 °C

With pyridine; lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1039/b006113l