C₄₄H₆₀N₄O₃₀P₂S

Base Information

Chemical Name:C₄₄H₆₀N₄O₃₀P₂S
CAS No.:1054637-16-9
Molecular Formula:C₄₄H₆₀N₄O₃₀P₂S
Molecular Weight:1218.98
Hs Code.:

C<sub>44</sub>H<sub>60</sub>N<sub>4</sub>O<sub>30</sub>P<sub>2</sub>S

Synonyms:

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Chemical Property of C₄₄H₆₀N₄O₃₀P₂S

Chemical Property:

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Technology Process of C₄₄H₆₀N₄O₃₀P₂S

There total 19 articles about C₄₄H₆₀N₄O₃₀P₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914642-50-5
benzyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-(D-1-{[2-(phenylsulfonyl)ethoxy]carbonyl}ethyl)-α-D-glucopyranoside

: 1054637-16-9
C₄₄H₆₀N₄O₃₀P₂S

Guidance literature:: Multi-step reaction with 8 steps

1: 55 percent / 4 Angstroem molecular sieves; AgOTf / CH₂Cl₂

2: ZnCl₂; AcOH

3: 2.1 g / AcOH; Zn / tetrahydrofuran

4: 92 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 2 h / 20 °C

5: tetrazole / acetonitrile / 4 h / 20 °C

6: 1.5 g / aq. hydrogen peroxide / tetrahydrofuran / 2 h / -80 - 20 °C

7: 72 percent / H₂ / Pd/C / methanol / 2 h / 20 °C / atmospheric pressure

8: pyridine; tertrazole / acetonitrile / 48 h / 20 °C

With pyridine; 1H-tetrazole; 4 A molecular sieve; hydrogen; dihydrogen peroxide; silver trifluoromethanesulfonate; acetic acid; zinc(II) chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1135/cccc20051615

Reference yield:

: 78246-81-8
benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 1054637-16-9
C₄₄H₆₀N₄O₃₀P₂S

Guidance literature:: Multi-step reaction with 11 steps

1.1: NaH / dioxane / 2 h / 95 °C

1.2: 80 percent / dioxane / 3 h / 60 °C

2.1: 84 percent / DMAP; EDCl / CH₂Cl₂

3.1: 91 percent / triflic acid; triethylsilane / CH₂Cl₂ / 1 h / -78 °C

4.1: 55 percent / 4 Angstroem molecular sieves; AgOTf / CH₂Cl₂

5.1: ZnCl₂; AcOH

6.1: 2.1 g / AcOH; Zn / tetrahydrofuran

7.1: 92 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 2 h / 20 °C

8.1: tetrazole / acetonitrile / 4 h / 20 °C

9.1: 1.5 g / aq. hydrogen peroxide / tetrahydrofuran / 2 h / -80 - 20 °C

10.1: 72 percent / H₂ / Pd/C / methanol / 2 h / 20 °C / atmospheric pressure

11.1: pyridine; tertrazole / acetonitrile / 48 h / 20 °C

With pyridine; 1H-tetrazole; triethylsilane; dmap; trifluorormethanesulfonic acid; 4 A molecular sieve; hydrogen; dihydrogen peroxide; silver trifluoromethanesulfonate; sodium hydride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1135/cccc20051615

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 1054637-16-9
C₄₄H₆₀N₄O₃₀P₂S

Guidance literature:: Multi-step reaction with 13 steps

1.1: 70 percent / AcCl / CH₂Cl₂ / 4 h / 75 °C

2.1: 95 percent / p-toluenesulfonic acid; triethyl ortoformate / dimethylformamide; dioxane / 20 h / 20 °C

3.1: NaH / dioxane / 2 h / 95 °C

3.2: 80 percent / dioxane / 3 h / 60 °C

4.1: 84 percent / DMAP; EDCl / CH₂Cl₂

5.1: 91 percent / triflic acid; triethylsilane / CH₂Cl₂ / 1 h / -78 °C

6.1: 55 percent / 4 Angstroem molecular sieves; AgOTf / CH₂Cl₂

7.1: ZnCl₂; AcOH

8.1: 2.1 g / AcOH; Zn / tetrahydrofuran

9.1: 92 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 2 h / 20 °C

10.1: tetrazole / acetonitrile / 4 h / 20 °C

11.1: 1.5 g / aq. hydrogen peroxide / tetrahydrofuran / 2 h / -80 - 20 °C

12.1: 72 percent / H₂ / Pd/C / methanol / 2 h / 20 °C / atmospheric pressure

13.1: pyridine; tertrazole / acetonitrile / 48 h / 20 °C

With pyridine; 1H-tetrazole; triethylsilane; dmap; trifluorormethanesulfonic acid; 4 A molecular sieve; hydrogen; dihydrogen peroxide; silver trifluoromethanesulfonate; sodium hydride; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; orthoformic acid triethyl ester; zinc(II) chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1135/cccc20051615