[Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂]

Base Information

Chemical Name:[Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂]
CAS No.:1257333-50-8
Molecular Formula:C₅₆H₃₂CuN₈
Molecular Weight:880.47
Hs Code.:

[Cu(NC<sub>4</sub>H<sub>2</sub>)3(C(C<sub>6</sub>H<sub>5</sub>))4NC<sub>4</sub>N<sub>2</sub>C<sub>12</sub>H<sub>6</sub>N<sub>2</sub>]

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Chemical Property of [Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂]

Chemical Property:

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Technology Process of [Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂]

There total 6 articles about [Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₆H₃₄N₈

: 1257333-50-8
[Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂]

Guidance literature:: C₅₆H₃₄N₈; With copper diacetate; In methanol; dichloromethane; for 12h; Inert atmosphere; Reflux;

With sodium acetate; edetate disodium; acetic acid; In dichloromethane; water; at 20 ℃; for 24h; pH=4.7;
DOI:10.1016/j.ica.2010.07.008

Reference yield:

: 14172-91-9
(tetraphenylporphyrin)copper(II)

: 1257333-50-8
[Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂]

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic anhydride; copper(II) nitrate / dichloromethane / 20 h / 20 °C / Inert atmosphere

2.1: sulfuric acid / dichloromethane / 0.13 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride; tin(ll) chloride / dichloromethane; water / 0.5 h / 60 °C / Inert atmosphere; Microwave irradiation

3.2: 1 h / Inert atmosphere; UV-irradiation

4.1: trifluoroacetic acid / dichloromethane / 24 h / Inert atmosphere; Reflux

5.1: copper diacetate / methanol; dichloromethane / 12 h / Inert atmosphere; Reflux

5.2: 24 h / 20 °C / pH 4.7

With hydrogenchloride; sulfuric acid; copper diacetate; acetic anhydride; copper(II) nitrate; trifluoroacetic acid; tin(ll) chloride; In methanol; dichloromethane; water;
DOI:10.1016/j.ica.2010.07.008

Reference yield:

: 71147-55-2
Cu(2+)-nitro-α,β,γ,δ-tetraphenylporphine

: 1257333-50-8
[Cu(NC₄H₂)3(C(C₆H₅))4NC₄N₂C₁₂H₆N₂]

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / dichloromethane / 0.13 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride; tin(ll) chloride / dichloromethane; water / 0.5 h / 60 °C / Inert atmosphere; Microwave irradiation

2.2: 1 h / Inert atmosphere; UV-irradiation

3.1: trifluoroacetic acid / dichloromethane / 24 h / Inert atmosphere; Reflux

4.1: copper diacetate / methanol; dichloromethane / 12 h / Inert atmosphere; Reflux

4.2: 24 h / 20 °C / pH 4.7

With hydrogenchloride; sulfuric acid; copper diacetate; trifluoroacetic acid; tin(ll) chloride; In methanol; dichloromethane; water;
DOI:10.1016/j.ica.2010.07.008