Technology Process of C58H86N6O10
There total 9 articles about C58H86N6O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
tetrahydrofuran; water;
at 20 ℃;
for 48h;
DOI:10.1021/ja109665t
- Guidance literature:
-
Multi-step reaction with 6 steps
1: methanol; N-ethyl-N,N-diisopropylamine / 20 °C / Inert atmosphere
2: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C
3: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
4: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
5: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
6: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
With
methanol; water; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; lithium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1021/ja109665t
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C
2: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
3: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
4: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
5: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
With
water; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; lithium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1021/ja109665t