Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester

Base Information

• Chemical Name: Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester
• CAS No.: 134353-82-5
• Molecular Formula: C₃₂H₄₄O₈SSi
• Molecular Weight: 616.848

Synonyms:

Chemical Property of Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester

There total 2 articles about Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

acetic anhydride (108-24-7) + 5-S-acetyl-3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3,5-dideoxy-1,2-O-isopropylidene-5-thio-α-D-ribofuranose (134353-80-3) → Acetic acid (2S,3R,4S,5S)-2-acetoxy-5-acetylsulfanylmethyl-4-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-tetrahydro-furan-3-yl ester (134353-81-4) + Acetic acid (1S,2S)-2-((4R,5S)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester (134353-82-5,134353-83-6) + Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester (134353-82-5,134353-83-6)

Guidance literature:

With camphor-10-sulfonic acid; In acetic acid; at 15 ℃; for 24h;

DOI:10.1016/0008-6215(91)80095-5

Reference yield: 8.0%

acetic anhydride (108-24-7) + 5-S-acetyl-3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3,5-dideoxy-1,2-O-isopropylidene-5-thio-α-D-ribofuranose (134353-80-3) → Acetic acid (2S,3R,4S,5S)-2-acetoxy-5-acetylsulfanylmethyl-4-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-tetrahydro-furan-3-yl ester (134353-81-4) + Acetic acid (1S,2S)-2-((4R,5S)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester (134353-82-5,134353-83-6) + Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester (134353-82-5,134353-83-6)

Guidance literature:

With camphor-10-sulfonic acid; In acetic acid; at 15 ℃; for 24h;

DOI:10.1016/0008-6215(91)80095-5

upstream raw materials:

acetic anhydride

5-S-acetyl-3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3,5-dideoxy-1,2-O-isopropylidene-5-thio-α-D-ribofuranose

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 134353-82-5 Acetic acid (1S,2S)-2-((4R,5R)-5-acetoxy-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-acetylsulfanylmethyl-4-(tert-butyl-diphenyl-silanyloxy)-butyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send