RuH₆(P(C₆H₅)3)2

Base Information

• Chemical Name: RuH₆(P(C₆H₅)3)2
• CAS No.: 87800-34-8
• Molecular Formula: C₃₆H₃₆P₂Ru
• Molecular Weight: 631.699

Synonyms:

Chemical Property of RuH₆(P(C₆H₅)3)2

Chemical Property:

Purity/Quality:

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Technology Process of RuH₆(P(C₆H₅)3)2

There total 2 articles about RuH₆(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(styrene)bis(triphenylphosphine)ruthenium(0) (68088-93-7) → RuH6(P(C6H5)3)2 (87800-34-8) + Ru2H6(P(C6H5)3)4 (97570-07-5)

Guidance literature:

With H₂; In hexane; H2 bubbling through a susp. of the complex for 2 h with stirring, colorchanging from purple to brown, a pink ppt. filtering off, drying in vacuo; a mixt. of mono- and dinuclear complexes was obtained with a total yield 75%; not isolated, identified by IR and NMR spectra;

DOI:10.1021/om00129a006

Reference yield:

bis(styrene)bis(triphenylphosphine)ruthenium(0) (68088-93-7) → RuH6(P(C6H5)3)2 (87800-34-8) + Ru2H8(P(C6H5)3)4

Guidance literature:

With H₂; In hexane; pptn. during reaction; product mixt. not sepd., detd. by IR and NMR spectroscopy;

DOI:10.1039/c39830000641

Reference yield: 20.0%

RuH6(P(C6H5)3)2 (87800-34-8) + Ru2H6(P(C6H5)3)4 (97570-07-5) → Ru2H4N2(P(C6H5)3)4

Guidance literature:

With N₂; In toluene; a mixt. of mono- and dinuclear complexes dissolving in toluene at 50°C under N2, hexane adding to a resulting red soln., filtering, cooling to -15°C, allowing to stand for 2 weeks; identified by elem. anal., NMR spectra and single crystal X-ray diffraction;

DOI:10.1021/om00129a006

upstream raw materials:

bis(styrene)bis(triphenylphosphine)ruthenium⁽⁰⁾

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