dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron

Base Information

Chemical Name:dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron
CAS No.:125979-20-6
Molecular Formula:C₂₉H₃₅FeNO₈P₂
Molecular Weight:643.393
Hs Code.:

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Chemical Property of dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron

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Technology Process of dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron

There total 3 articles about dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 5110-45-2,73940-93-9
diphenylketene-N-p-tolylimine

: 79110-70-6
mu.-dinitrogenbis(dicarbonylbis(trimethylphosphite)iron)

: 125979-20-6
dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron

Guidance literature:: In diethyl ether; byproducts: N2; under Ar or N2, addn. of Ph2C2N-p-tolyl in ether to a soln. of Fe-compd. in ether at -30°C, slow warmed to room temp., stirred for 20 h; removal of solvent by evapn., extn. (ether, 30°C), filtered, cooled to -40°C for 3 d; elem. anal.;
DOI:10.1016/0022-328X(89)87232-8

Reference yield:

: 52155-11-0,1174574-37-8,26623-61-0
(CO)2Fe{P(OCH₃)3}2I₂

: 125979-20-6
dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron

Guidance literature:: Multi-step reaction with 3 steps

1: sodium; CO / diethyl ether

2: nitrogen / diethyl ether

3: diethyl ether

With sodium; CO; nitrogen; In diethyl ether;
DOI:10.1016/0022-328X(89)87232-8

Reference yield:

: 19457-84-2,14949-85-0
tricarbonylbis(trimethylphosphite)iron

: 125979-20-6
dicarbonylbis(trimethylphosphite)diphenyl-p-tolylketene imine iron

Guidance literature:: Multi-step reaction with 2 steps

1: nitrogen / diethyl ether

2: diethyl ether

With nitrogen; In diethyl ether;
DOI:10.1016/0022-328X(89)87232-8