PhNHCOCH(COMe)CONHPh

Base Information

• Chemical Name: PhNHCOCH(COMe)CONHPh
• CAS No.: 72600-16-9
• Molecular Formula: C₁₇H₁₆N₂O₃
• Molecular Weight: 296.326

Synonyms:

Chemical Property of PhNHCOCH(COMe)CONHPh

Chemical Property:

Purity/Quality:

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Technology Process of PhNHCOCH(COMe)CONHPh

There total 3 articles about PhNHCOCH(COMe)CONHPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(PhNCO)2CCOMe]Na → PhNHCOC(CONHPh)C(OH)Me + PhNHCOCH(COMe)CONHPh (72600-16-9)

Guidance literature:

With hydrogenchloride; In N,N-dimethyl-formamide;

DOI:10.1002/poc.1611

Reference yield:

aniline (62-53-3) + diethyl 1,3-acetonedicarboxylate (105-50-0) → 2-acetyl-N-phenyl-malonamic acid ethyl ester (18629-86-2) + PhNHCOCH(COMe)CONHPh (72600-16-9) + 3-anilino-4-phenylcarbamoyl-crotonic acid ethyl ester

Guidance literature:

at 100 ℃; im Druckrohr;

Reference yield:

→ PhNHCOCH(COMe)CONHPh (72600-16-9)

Guidance literature:

entspr. β-Dicarbonyl, Ni(acac)2, PhNCO, CH2Cl2;

upstream raw materials:

aniline

diethyl 1,3-acetonedicarboxylate

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