5,10,15,20-tetrakis[4-(11-methoxycarbonylundecane-1-oxy)phenyl]porphyrinato zinc(II)

Base Information

Chemical Name:5,10,15,20-tetrakis[4-(11-methoxycarbonylundecane-1-oxy)phenyl]porphyrinato zinc(II)
CAS No.:871466-63-6
Molecular Formula:C₉₆H₁₂₄N₄O₁₂Zn
Molecular Weight:1591.45
Hs Code.:

Synonyms:

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Chemical Property of 5,10,15,20-tetrakis[4-(11-methoxycarbonylundecane-1-oxy)phenyl]porphyrinato zinc(II)

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Technology Process of 5,10,15,20-tetrakis[4-(11-methoxycarbonylundecane-1-oxy)phenyl]porphyrinato zinc(II)

There total 1 articles about 5,10,15,20-tetrakis[4-(11-methoxycarbonylundecane-1-oxy)phenyl]porphyrinato zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.7%

: 109-97-7,30604-81-0
pyrrole

: 871360-91-7
OHCC₆H₄OC₁₁H₂₂COOCH₃

: 5970-45-6
zinc(II) acetate dihydrate

: 118-75-2
chloranil

: 871466-63-6
5,10,15,20-tetrakis[4-(11-methoxycarbonylundecane-1-oxy)phenyl]porphyrinato zinc(II)

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; pyrrole, OHCC6H4OC11H22COOCH3 and Zn(CH3COO)2*2H2O added to CHCl3, purged with Ar for 30 min; BF3*O(C2H5)2 added; Ar introduced for 10 min; mixt. stirred at 30°C for 3.5 h; p-chloranil added; mixt. refluxed for 1 h; washed (satd. NaHCO3 aq. and water); dried over Na2SO4; silica gel added; solvent removed by evapn.; ppt. (CH2Cl2/CH3OH);
DOI:10.1016/j.electacta.2005.05.030