Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Base Information

Chemical Name:Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄
CAS No.:752245-69-5
Molecular Formula:C₃₈H₅₅F₆IrO₂P₂
Molecular Weight:912.011
Hs Code.:

Ir(C<sub>6</sub>H<sub>2</sub>(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>(OP(C(CH<sub>3</sub>)3)2)2)C<sub>8</sub>H<sub>14</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Chemical Property:

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Technology Process of Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

There total 3 articles about Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 671789-64-3
IrHCl(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)

: 292-64-8
Cyclooctan

: 686274-20-4
[p-(3,5-CF₃)2C₆H₃C₆H₂-2,6-(OP(tBu)2)2]IrH₂

: 752245-69-5
Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Guidance literature:: With sodium t-butanolate; In neat (no solvent); byproducts: NaCl, OHC(CH3)3; Sonication; cyclooctane and cyclooctene were added to mixt. of Ir-complex and NaOC(CH3)3 under Ar, shaken and treated with ultrasound for 30-60 min at 23°C;
DOI:10.1021/ja048393f

Reference yield:

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 686274-20-4
[p-(3,5-CF₃)2C₆H₃C₆H₂-2,6-(OP(tBu)2)2]IrH₂

: 292-64-8
Cyclooctan

: 752245-69-5
Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Guidance literature:: In neat (no solvent); Ir-complex was reacted with cyclooctane and cyclooctene at 23°C;
DOI:10.1021/ja048393f

Reference yield:

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 686274-20-4
[p-(3,5-CF₃)2C₆H₃C₆H₂-2,6-(OP(tBu)2)2]IrH₂

: 752245-69-5
Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Guidance literature:: In further solvent(s); soln. of Ir-complex in methylcyclohexane-d14 was cooled to -125°C, soln. of cyclooctene in methylcyclohexane-d14 was added, mixed at -110°C, shimmed, heated at -70°C; monitored by NMR;
DOI:10.1021/ja048393f