tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid

Base Information

Chemical Name:tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid
CAS No.:129729-28-8
Molecular Formula:C₈₃H₈₆O₁₉Si
Molecular Weight:1415.67
Hs Code.:

tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid

Synonyms:

Suppliers and Price of tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid

There total 2 articles about tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 129729-29-9
O-(methyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyluronate)-(1->4)-O-(methyl 2,3-di-O-benzyl-α-D-galactopyranosyluronate)-(1->4)-

: (4S,5R,6S)-4,5-Bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxy)-5,6-dihydro-4H-pyran-2-carboxylic acid methyl ester

: 129729-28-8
tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid

Guidance literature:: With lithium iodide; In pyridine; for 7h; Heating;
DOI:10.1016/0008-6215(90)84203-7

Reference yield:

: 129729-27-7
tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranoside

: 129729-28-8
tert-butyldiphenylsilyl O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyluronic acid)-(1->4)-O-(2,3-di-O-benzyl-α-D-galactopyranosyluronic acid)-(1->4)-2,3-di-O-benzyl-β-D-galactopyranosiduronic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; dimethyl sulfoxide; Yield given. Multistep reaction; 1.) CH₂Cl₂, -78 deg, 30 min, 2.) t-BuOH, H₂O;
DOI:10.1016/0008-6215(90)84203-7