Technology Process of tetracyclo<4.2.2.12,5.02,6>undecan-3-on-(p-toluolsulfonylhydrazone)
There total 5 articles about tetracyclo<4.2.2.12,5.02,6>undecan-3-on-(p-toluolsulfonylhydrazone) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
for 2h;
Heating;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) B2H6, 2) 30percent H2O2, aq. NaOH / 1a) 1 h, 0 deg C, ether, THF, 1b) 1 h, room temperature, 2) 1 h, room temperature
2: sodium dichromate, 97percent H2SO4 / H2O; diethyl ether / 2 h / Ambient temperature
3: 63 percent / methanol. HCl / 2 h / Heating
With
hydrogenchloride; sodium hydroxide; sodium dichromate; sulfuric acid; dihydrogen peroxide; diborane;
In
diethyl ether; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) Et4NBr / 1) DMF, -20 deg C, mercury cathode, platinum-net anode, 100 mA, 2a) -20 deg C, 30 min, 2b) 3 h, 0 deg C, 2c) 16 h, room temperature
2: 1) B2H6, 2) 30percent H2O2, aq. NaOH / 1a) 1 h, 0 deg C, ether, THF, 1b) 1 h, room temperature, 2) 1 h, room temperature
3: sodium dichromate, 97percent H2SO4 / H2O; diethyl ether / 2 h / Ambient temperature
4: 63 percent / methanol. HCl / 2 h / Heating
With
hydrogenchloride; sodium hydroxide; sodium dichromate; sulfuric acid; tetraethylammonium bromide; dihydrogen peroxide; diborane;
In
diethyl ether; water;
