Technology Process of C41H47N3O7
There total 5 articles about C41H47N3O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; potassium iodide;
In
N,N-dimethyl-formamide;
at 4 - 20 ℃;
for 48h;
DOI:10.1021/jm400823w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 3 h / 4 - 20 °C
2: sodium tris(acetoxy)borohydride; acetic acid / 16 h / 20 °C
3: potassium iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 4 - 20 °C
With
sodium tris(acetoxy)borohydride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium iodide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm400823w
- Guidance literature:
-
Multi-step reaction with 5 steps
1: caesium carbonate / N,N-dimethyl-formamide / 20 °C
2: toluene-4-sulfonic acid / ethyl acetate; ethanol / 2 h / 0 - 20 °C
3: triethylamine / dichloromethane / 3 h / 4 - 20 °C
4: sodium tris(acetoxy)borohydride; acetic acid / 16 h / 20 °C
5: potassium iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 4 - 20 °C
With
sodium tris(acetoxy)borohydride; caesium carbonate; toluene-4-sulfonic acid; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium iodide;
In
ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm400823w
