C₂₉H₃₃F₃N₆O₄S

Base Information

Chemical Name:C₂₉H₃₃F₃N₆O₄S
CAS No.:1332380-76-3
Molecular Formula:C₂₉H₃₃F₃N₆O₄S
Molecular Weight:618.68
Hs Code.:

C<sub>29</sub>H<sub>33</sub>F<sub>3</sub>N<sub>6</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₂₉H₃₃F₃N₆O₄S

Chemical Property:

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Technology Process of C₂₉H₃₃F₃N₆O₄S

There total 13 articles about C₂₉H₃₃F₃N₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₃₇F₃N₆O₄S

: 1332380-76-3
C₂₉H₃₃F₃N₆O₄S

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃;
DOI:10.1016/j.bmcl.2012.08.111

Reference yield:

: 168958-14-3
C₁₅H₂₅NO₆

: 1332380-76-3
C₂₉H₃₃F₃N₆O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran / 1 h / -30 °C

2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / ethanol / 1.5 h / 120 °C

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / N,N-dimethyl-formamide / 2 h / 110 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C

6: 1,4-dioxane / 16 h / 120 °C

7: hydrogenchloride / tetrahydrofuran; water / 0 °C

With hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.08.111

Reference yield:

: 1208988-90-2
C₁₇H₁₉NO₅

: 1332380-76-3
C₂₉H₃₃F₃N₆O₄S

Guidance literature:: Multi-step reaction with 10 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 16 h / 20 °C

2: tetrahydrofuran / 1 h / -78 °C

3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 16 h / 20 °C

4: tetrahydrofuran / 2 h / -78 °C

5: hydrazine hydrate / ethanol / 2 h / 70 °C

6: N-ethyl-N,N-diisopropylamine / ethanol / 1.5 h / 120 °C

7: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / N,N-dimethyl-formamide / 2 h / 110 °C

8: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C

9: 1,4-dioxane / 16 h / 120 °C

10: hydrogenchloride / tetrahydrofuran; water / 0 °C

With hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; caesium carbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.08.111