Technology Process of C27H25ClO8
There total 13 articles about C27H25ClO8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; water;
In
tetrahydrofuran; methanol;
at 50 ℃;
for 16h;
DOI:10.1002/chem.201402254
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C
2.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere
2.2: 0.33 h
3.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere
4.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C
With
hydrogenchloride; dmap; water; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1002/chem.201402254
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 20 h / 65 °C / Inert atmosphere
2.1: sodium acetate; acetic acid / 12 h / 80 °C / Inert atmosphere
3.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C
4.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere
4.2: 0.33 h
5.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere
6.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C
With
hydrogenchloride; dmap; water; sodium acetate; toluene-4-sulfonic acid; acetic acid; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;
DOI:10.1002/chem.201402254
